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HRID 329333作成日:2026年10月26日

Calcium Chloride → HCID 21439120、化合物

https://huagongshe.com/reaction/329333

反応式

関与物質

役割名称HCID仕込み量
反応物Calcium ChlorideHCID 5284359—
反応物sodium 2-(5-oxo-5H-dibenzo[a,d]cyclohepten-2-yl)propionateHCID 23670418—
溶媒WaterHCID 962—
生成物HCID 21439120HCID 21439120—

反応手順

25.2 G. of sodium 2-(5-oxo-5H-dibenzo[a,d]cyclohepten-2-yl)propionate in 300 ml. of water is added to a mixture of 5.55 g. of calcium chloride in 300 ml. of water, and the mixture is allowed to stand for 12 hrs. at room temperature. The mixture is then filtered, and the filtered salt washed several times with portions of ice cold water. The washed salt is dried under vacuum to yield calcium 2-(5-oxo-5H-dibenzo[a,d]cyclohepten-2-yl)propionate.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04020094
出典データセットuspto-grants-1977_04
ORD IDord-5b5b2fc142994dc49ee144bd0c4aa90e
出典メモuspto-grants-1977_04