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Benzyl Bromide → 1-(Phenylmethyl)pyrrolidine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzyl Bromide | HCID 7498 | — |
| 反応物 | Pyrrolidine | HCID 31268 | — |
| 溶媒 | Diethyl Ether | HCID 3283 | — |
| 生成物 | 1-(Phenylmethyl)pyrrolidine | HCID 122501 | — |
反応手順
A 25.0 ml portion of pyrrolidine was reacted with 10.9 ml of benzyl bromide in ether as described in Example 3, giving 12.3 g of 1-(phenylmethyl)pyrrolidine, which was then reacted with butyl lithium and diphenylphosphine chloride as described in Example 3, giving diphenyl]2-(1-pyrrolidinylmethyl)phenyl]phosphine.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04892885 |
| 出典データセット | uspto-grants-1990_01 |
| ORD ID | ord-9293d2e303a2441eba00c7ae2796c964 |
| 出典メモ | uspto-grants-1990_01 |