関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | 1,1,3,3-Tetramethyl-disiloxane | HCID 18659 | — |
| 反応物 | N-Allylcyclohexylamine | HCID 81115 | — |
| 触媒 | Chloroplatinic acid | HCID 61859 | — |
| 生成物 | 1,3-bis(N-cyclohexyl-3-aminopropyl)-1,1,3,3-tetramethyldisiloxane | HCID 19871404 | — |
反応手順
Following the technique described in Example 1, N-allylcyclohexylamine (0.173 mole), 1,1,3,3-tetramethyldisiloxane (0.0783 mole), and 0.05 g hexachloroplatinic acid are stirred at 70° C for eight hours at 110° C. under nitrogen. The product, in nearly quantitative yield, is purified by vacuum distillation at <1 torr at a temperature of 207°-210° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04892918 |
|---|
| 出典データセット | uspto-grants-1990_01 |
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| ORD ID | ord-c0289677df37416ba173f315dea44ca7 |
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| 出典メモ | uspto-grants-1990_01 |
|---|
