2-Methyl-4-amino-5-aminomethylpyrimidine carbonate → 4-Amino-2-methyl-5-pyrimidinemethanamine
反応式
C(=O)(O)O.[CH3:5][C:6]1[N:11]=[C:10]([NH2:12])[C:9]([CH2:13][NH2:14])=[CH:8][N:7]=1>C(O)(C)C>[CH3:5][C:6]1[N:11]=[C:10]([NH2:12])[C:9]([CH2:13][NH2:14])=[CH:8][N:7]=1参加物
3
反応条件
- 温度
- 85 °C
実験手順
An amount of 170 g of isopropanol was added to 30.0 g of the 2-methyl-4-amino-5-aminomethylpyrimidine carbonate thus obtained, followed by heating at about 85° C. for 180 minutes to give 2-methyl-4-amino-5-aminomethylpyrimidine with purity of 99.0%.
後処理
- customthus obtained
出典と根拠
- ORDレコード
- ord-daebf62d6a7d48fa849fe817df70603a
- 出典データセット
- uspto-grants-1990_01
- 特許番号
- US04892948
反応ノート
読み込み中…