化工社化工社 化学情報印刷レポート · 研究参考用
Perchlorate → Phenylphosphine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Perchlorate | HCID 123351 | — |
| 反応物 | 1-Methylphenylphosphanium carbonate | HCID 86743659 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Phenylphosphine | HCID 12519 | — |
| 生成物 | Methylphosphanium perchlorate | HCID 19871530 | — |
反応手順
By following the same procedure as the 2nd step of Example 12 except that 10.0 g of 1-methylphenylphosphanium carbonate, 6.9 g of 60% perchlorate, and 10.0 g of water were used, 10.9 g (94.8% of the theoretical yield, yield of 67.6% to 1-phenylphosphane) of methylphosphanium perchlorate was obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04892944 |
| 出典データセット | uspto-grants-1990_01 |
| ORD ID | ord-f1dfed6d36574850a6245e0f377c767f |
| 出典メモ | uspto-grants-1990_01 |