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HRID 330232作成日:2026年10月24日

Lauric Acid → N-(2-Methoxy-5-pyridyl)-cyclopropane carboxamide dodecanoic acid salt

https://huagongshe.com/ja/reaction/330232

反応式

関与物質

役割名称HCID仕込み量
反応物Lauric AcidHCID 3893—
反応物N-(6-methoxypyridin-3-yl)cyclopropanecarboxamideHCID 86308—
溶媒AcetoneHCID 180—
生成物N-(2-Methoxy-5-pyridyl)-cyclopropane carboxamide dodecanoic acid saltHCID 14304482—

反応手順

Three grams (0.016 mole) of the compound of Example 1 was dissolved in 100 ml of acetone in a 300 ml, one-neck, round-bottom flask by swirling. 3.2 g (0.016 mole) dodecanoic acid was added which went into solution. The resulting solution was evaporated on a rotary evaporator, yielding 6.2 g, of a white solid having a melting point of 92°-96° C., which was identified by nuclear magnetic resonance spectroscopy as the title compound. This compound will be known as Compound 7.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04895858
出典データセットuspto-grants-1990_01
ORD IDord-5ac46be8efc64a7882dd6352e59966b7
出典メモuspto-grants-1990_01