化工社化工社 化学情報印刷レポート · 研究参考用
Tetrafluoro-m-phenylenediamine dihydrochloride → n-(2-Pyrid-2-ylethyl)benzene-1,4-diamine dihydrochloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Tetrafluoro-m-phenylenediamine dihydrochloride | HCID 149026 | — |
| 反応物 | 2-[2-(4-Nitroanilino)ethyl]pyridine | HCID 13301713 | — |
| 触媒 | ZINC ammonium chloride water ethanol | HCID 131726756 | — |
| 生成物 | n-(2-Pyrid-2-ylethyl)benzene-1,4-diamine dihydrochloride | HCID 69214213 | — |
反応手順
The N-(4-nitrophenyl)-N-(2-pyrid-2-ylethyl)amine (5) obtained above was reduced with a boiling zinc/ammonium chloride/water/ethanol mixture. The corresponding amine was isolated in dihydrochloride form.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07429278B2 |
| 出典データセット | uspto-grants-2008_09 |
| ORD ID | ord-fe6fe9f925824fb6aea92d62733bbd4f |
| 出典メモ | uspto-grants-2008_09 |