化工社化工社 化学情報印刷レポート · 研究参考用
Benzylamine → GlyTouCan:G63996AI
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzylamine | HCID 7504 | — |
| 反応物 | beta-D-Galactose pentaacetate | HCID 94752 | — |
| 溶媒 | Tetrahydrofuran | HCID 8028 | — |
| 生成物 | GlyTouCan:G63996AI | HCID 11152232 | — |
反応手順
The synthesis of compound 9 is illustrated in FIG. 6. 20 g (51.24 mmol) of β-D-galactosepentaacetate 1 was dissolved in 150 ml THF and 6.7 ml (61.49 mmol) of benzylamine was added with a dropping funnel. The reaction was stirred for 18 h at room temperature to give 2,3,4,6-tetra-O-acetyl-β-D-galactopyranose 2.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08877917B2 |
| 出典データセット | uspto-grants-2014_11 |
| ORD ID | ord-9208ea680a3d4041996f1373e850ba66 |
| 出典メモ | uspto-grants-2014_11 |