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HRID 333020作成日:2026年10月26日

Methyl iodide → HCID 178480658、化合物

https://huagongshe.com/reaction/333020

反応式

関与物質

役割名称HCID仕込み量
反応物Methyl iodideHCID 6328—
反応物1-(4-Chlorophenyl)-1H-imidazoleHCID 142859—
溶媒TetrahydrofuranHCID 8028—
生成物HCID 178480658HCID 178480658—

反応手順

1-(4-Chlorophenyl)imidazole (0.37 g, 2.07 mmol) is dissolved in THF (5 ml) and subsequently admixed with methyl iodide (1.47 g, 10.4 mmol) and allowed to stand for 20 hours. The precipitate formed is subsequently filtered off and washed with ethanol and with petroleum ether and subsequently dried under reduced pressure. This gives 0.46 g of 1-(4-chlorophenyl)-3-methylimidazolium iodide.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US08877937B2
出典データセットuspto-grants-2014_11
ORD IDord-676487415dcd4a69a0c42a1697107604
出典メモuspto-grants-2014_11