3-formyl-N,N-dimethylbenzene-1-sulfonamide → 4-Formyl-N-methylbenzenesulfonamide

HRID 333037ノート

反応式

HRID 333037 の反応式
C([C:3]1[CH:4]=[C:5]([S:9]([N:12]([CH3:14])C)(=[O:11])=[O:10])[CH:6]=[CH:7][CH:8]=1)=O.C(NS(C1C=CC=C([CH:27]=[O:28])C=1)(=O)=O)C.C(C1C=C(S(NCCC)(=O)=O)C=CC=1)=O.C(C1C=C(S(NC(C)C)(=O)=O)C=CC=1)=O>>[CH:27]([C:8]1[CH:3]=[CH:4][C:5]([S:9]([NH:12][CH3:14])(=[O:10])=[O:11])=[CH:6][CH:7]=1)=[O:28]

参加物

5

反応物 4

HCID 198159763-formyl-N,N-dimethylbenzene-1-sulfonamideHCID 86676515N-ethyl-3-formyl-benzenesulfonamideHCID 866765163-formyl-N-propyl-benzenesulfonamideHCID 866765173-formyl-N-isopropyl-benzenesulfonamide

生成物 1

HCID 143271774-Formyl-N-methylbenzenesulfonamide

実験手順

3-Formyl-N,N-dimethyl-benzenesulfonamide, N-ethyl-3-formyl-benzenesulfonamide, 3-formyl-N-propyl-benzenesulfonamide and 3-formyl-N-isopropyl-benzenesulfonamide were oils and were used without further purification in the next step of reaction.

後処理

  1. customwere used without further purification in the next step of reaction

出典と根拠

ORDレコード
ord-44f48bbac74f4f55ae5d2c5966139bb6
出典データセット
uspto-grants-2014_11
特許番号
US08877946B2

反応ノート

読み込み中…