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Isopropylamine → HCID 86699881、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Isopropylamine | HCID 6363 | — |
| 反応物 | Aminopropyltrimethoxysilane | HCID 83756 | — |
| 反応物 | 2,2-Dimethyl-3-(dimethylamino)propionaldehyde | HCID 84921 | — |
| 生成物 | HCID 86699881 | HCID 86699881 | — |
反応手順
13.57 g 2,2-dimethyl-3-dimethylaminopropanal, 7.45 g 2-propanamine and 17.93 g 3-aminopropyltrimethoxysilane were reacted according to the general manufacturing procedure (iminosilanes). The product was distilled after manufacture in order to remove oligomer portions. Yield: 28.4 g of a clear, colorless oil having an amine content of 6.61 mmol N/g and a purity of 95%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08877955B2 |
| 出典データセット | uspto-grants-2014_11 |
| ORD ID | ord-03e3e68b4236413386c8ac136302706a |
| 出典メモ | uspto-grants-2014_11 |