3-Bromoaniline → 1-(3-Bromo-phenyl)-1H-[1,2,4]-triazole-3-carboxylic acid

反応式

[Br:1][C:2]1[CH:3]=[C:4]([CH:6]=[CH:7][CH:8]=1)[NH2:5].C1(C)C=CC=C(N2[CH:19]=[N:18][C:17]([C:20]([OH:22])=[O:21])=[N:16]2)C=1>>[Br:1][C:2]1[CH:3]=[C:4]([N:5]2[CH:19]=[N:18][C:17]([C:20]([OH:22])=[O:21])=[N:16]2)[CH:6]=[CH:7][CH:8]=1

参加物

反応物 2

HCID 115623-Bromoaniline

HCID 713020901-(m-Tolyl)-1H-1,2,4-triazole-3-carboxylic acid

生成物 1

HCID 866882371-(3-Bromo-phenyl)-1H-[1,2,4]-triazole-3-carboxylic acid

実験手順

This intermediate was prepared from 3-bromoaniline in three steps according to the preparation of 1-m-tolyl-1H-[1,2,4]-triazole-3-carboxylic acid (Method B).

出典と根拠

ORDレコード: ord-5d8e31547e04408fa55cb513165051fc
出典データセット: uspto-grants-2014_11
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US08883789B2

反応ノート

読み込み中…