反応式
[NH2:1][C:2]1[CH:10]=[CH:9][C:5]2[N:6]=[CH:7][NH:8][C:4]=2[CH:3]=1.ClC1C=C(C=CC=1)[CH:15]=[O:16].[CH2:20]([N+]#[C-])[CH2:21][CH2:22][CH3:23].[O:26]([C:28]#[N:29])[K].[Cl-:30].[NH+]1C=C[CH:34]=[CH:33][CH:32]=1>>[NH:6]1[C:5]2[CH:9]=[CH:10][C:2]([N:1]3[CH:23]([C:22]4[CH:34]=[CH:33][CH:32]=[C:20]([Cl:30])[CH:21]=4)[C:28](=[O:26])[NH:29][C:15]3=[O:16])=[CH:3][C:4]=2[N:8]=[CH:7]1参加物
6
実験手順
The compound was synthesized starting from 5-aminobenzimidazole 2.13 g (16 mmol), 3-chlorobenzaldehyde 2.24 g (16 mmol), n-butyl isonitrile 1.69 ml (16 mmol), KOCN 1.3 g (16 mmol) and pyridiniumchloride 1.85 g (16 mmol) as described in method 1.
後処理
- customThe compound was synthesized
出典と根拠
- ORDレコード
- ord-c1f91fad228748d59ff25171ad2b471d
- 出典データセット
- uspto-grants-2014_11
- 特許番号
- US08889709B2
関連ノート
読み込み中…