化工社化工社 化学情報印刷レポート · 研究参考用
4-Fluoro-2-nitrophenol → 2-Amino-4-fluorophenol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Fluoro-2-nitrophenol | HCID 136236 | — |
| 触媒 | Palladium | HCID 23938 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | 2-Amino-4-fluorophenol | HCID 2735917 | 86.9% |
反応手順
300 mg of 4-fluoro-2-nitrophenol was dissolved in 3 ml of ethanol, and 120 mg of 10% palladium/carbon was added and stirred under hydrogen atmosphere at room temperature for 1 hour. After the insoluble matter was filtered off, the filtrate was distilled off under reduced pressure to yield 211 mg of the title compound.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08889727B2 |
| 出典データセット | uspto-grants-2014_11 |
| ORD ID | ord-3bdbe08535b049f4b504bdb13705ee74 |
| 出典メモ | uspto-grants-2014_11 |