戻る
化工社化工社 化学情報印刷レポート · 研究参考用
HRID 33818作成日:2026年10月25日

Formic Acid → HCID 178420610、化合物

https://huagongshe.com/reaction/33818

反応式

関与物質

役割名称HCID仕込み量
反応物Formic AcidHCID 284—
反応物AnilineHCID 6115—
反応物2,6-DiformylpyridineHCID 79485—
溶媒EthanolHCID 702—
生成物HCID 178420610HCID 178420610—

反応手順

2,6-pyridine dicarboxaldehyde (0.3071 g, 2.3 mmol) was added to a solution of aniline (0.5292 g, 5.7 mmol) in absolute ethanol (20 mL) at room temperature. 0.5 mL of formic acid was then added to the above solution. The mixture was stirred at room temperature for 65 hours. The product was filtered, washed with cold ethanol and dried in a vacuum oven (50° C.) overnight. Yield 0.2245 g (34.2%).

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US07429684B2
出典データセットuspto-grants-2008_09
ORD IDord-21efaacccac443d7a83aa3e70255ab54
出典メモuspto-grants-2008_09