化工社化工社 化学情報印刷レポート · 研究参考用
Formic Acid → HCID 178420610、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Formic Acid | HCID 284 | — |
| 反応物 | Aniline | HCID 6115 | — |
| 反応物 | 2,6-Diformylpyridine | HCID 79485 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | HCID 178420610 | HCID 178420610 | — |
反応手順
2,6-pyridine dicarboxaldehyde (0.3071 g, 2.3 mmol) was added to a solution of aniline (0.5292 g, 5.7 mmol) in absolute ethanol (20 mL) at room temperature. 0.5 mL of formic acid was then added to the above solution. The mixture was stirred at room temperature for 65 hours. The product was filtered, washed with cold ethanol and dried in a vacuum oven (50° C.) overnight. Yield 0.2245 g (34.2%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07429684B2 |
| 出典データセット | uspto-grants-2008_09 |
| ORD ID | ord-21efaacccac443d7a83aa3e70255ab54 |
| 出典メモ | uspto-grants-2008_09 |