3-Isopropylaniline → 3-bromo-N-(3-isopropylphenyl)-5-methylbenzamide

HRID 338742

反応式

HRID 338742 の反応式
[Br:1][C:2]1[CH:3]=[C:4]([CH:8]=[C:9]([CH3:11])[CH:10]=1)[C:5]([OH:7])=O.[CH:12]([C:15]1[CH:16]=[C:17]([CH:19]=[CH:20][CH:21]=1)[NH2:18])([CH3:14])[CH3:13]>>[Br:1][C:2]1[CH:3]=[C:4]([CH:8]=[C:9]([CH3:11])[CH:10]=1)[C:5]([NH:18][C:17]1[CH:19]=[CH:20][CH:21]=[C:15]([CH:12]([CH3:14])[CH3:13])[CH:16]=1)=[O:7]

参加物

3

反応物 2

HCID 4586793-IsopropylanilineHCID 34331273-Bromo-5-methylbenzoic acid

生成物 1

HCID 866958603-bromo-N-(3-isopropylphenyl)-5-methylbenzamide収率 99%

実験手順

In a manner similar to that described in Preparation 41, 3-bromo-5-methylbenzoic acid (400 mg) and 3-isopropylaniline were converted to the title compound (615 mg, 99%).

出典と根拠

ORDレコード
ord-569505674ad14816bf9f4b895934cad5
出典データセット
uspto-grants-2014_11
特許番号
US08889870B2

関連ノート

読み込み中…