化工社化工社 化学情報印刷レポート · 研究参考用
2-Amino-4-(trifluoromethyl)benzenethiol → HCID 68279297、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Amino-4-(trifluoromethyl)benzenethiol | HCID 88042 | — |
| 反応物 | HCID 86709921 | HCID 86709921 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | HCID 68279297 | HCID 68279297 | — |
反応手順
A solution including Compound 97c (1.0 eq.) and 2-amino-4-trifluoromethylbenzenethiol (1.0 eq.) was stirred in a methanol solvent at room temperature. After methanol was removed, the precipitate was filtered, and washed with cold methanol to obtain a solid target product.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08889881B2 |
| 出典データセット | uspto-grants-2014_11 |
| ORD ID | ord-b82717d95259479bb2385f249cfa8728 |
| 出典メモ | uspto-grants-2014_11 |