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Hydrochloric Acid → HCID 178418457、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | Cni H1894 | HCID 463010 | — |
| 反応物 | HCID 178418324 | HCID 178418324 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | HCID 178418457 | HCID 178418457 | — |
反応手順
Compound No. 12. A suspension of 3,5-diacetylaniline (0.531 g) in water (8 mL) was treated with cyanoguanidine (0.285 g) and conc. HCl (0.25 mL) and heated at reflux. After 6 hr the mixture was cooled and concentrated and 0.248 g of off-white solid was filtered out and dried to give N-(3,5-diacetylphenyl)biguanide hydrochloride, mp 260°-70° C. (dec).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05733932 |
| 出典データセット | uspto-grants-1998_03 |
| ORD ID | ord-705eb0cf3a5441248217ccc079f91152 |
| 出典メモ | uspto-grants-1998_03 |