化工社化工社 化学情報印刷レポート · 研究参考用
Sodium Hydroxide → Sodium 6-methoxynicotinate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | Methyl 6-methoxypyridine-3-carboxylate | HCID 586039 | — |
| 溶媒 | 1,4-Dioxane | HCID 31275 | — |
| 生成物 | Sodium 6-methoxynicotinate | HCID 23717611 | — |
反応手順
methyl 6-methoxynicotinate (2.097 g, 12.56 mmol) was dissolved in dioxane (30 mL). An aqueous solution of NaOH (1.0N, 25 mL) was added to the solution and the mixture was stirred at room temperature overnight. The solvent was removed under reduced pressure to provide 2.2 g of sodium 6-methoxynicotinate.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08895050B2 |
| 出典データセット | uspto-grants-2014_11 |
| ORD ID | ord-0482b300a3214a2a9e2d4a88299a8574 |
| 出典メモ | uspto-grants-2014_11 |