関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | (3R)-3-amino-3-phenylpropanoic acid | HCID 686703 | — |
| 反応物 | (3S)-3-amino-3-phenylpropanoic acid | HCID 686704 | — |
| 生成物 | L-Phenylalanine | HCID 6140 | — |
反応手順
The optical purity of (S)-β-phenylalanine was calculated from the peak area of the chromatogram obtained under analysis conditions illustrated in (1) above. Furthermore, the reaction yield of (S)-β-phenylalaninewas calculated from the peak area of the chromatogram obtained under analysis conditions illustrated in (2) above. Concretely, when the reaction solution contained a solid of β-phenylalanine or a solid of L-phenylalanine, a solution obtained by collecting a part of the reaction solution containing these solids, mixing with a 0.2 mol/l hydrochloric acid solution and dissolving these solids was analyzed. The amount (g) of (S)-β-phenylalanine synthesized was calculated from the peak area of the chromatogram using a calibration curve of (S)-β-phenylalanine standards to determine the yield from (Formula 1). Yield (%)=Amount of (S)-β-phenylalanine synthesized (g)/Amount of L-phenylalanine added (g)×100 (Formula 1)
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 特許番号 | US08895270B2 |
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| 出典データセット | uspto-grants-2014_11 |
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| ORD ID | ord-0819d9f57f5d4c14aba814481d948dd0 |
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| 出典メモ | uspto-grants-2014_11 |
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