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HRID 339440作成日:2026年10月26日

(3R)-3-amino-3-phenylpropanoic acid → L-Phenylalanine

https://huagongshe.com/reaction/339440

反応式

関与物質

役割名称HCID仕込み量
反応物(3R)-3-amino-3-phenylpropanoic acidHCID 686703—
反応物(3S)-3-amino-3-phenylpropanoic acidHCID 686704—
生成物L-PhenylalanineHCID 6140—

反応手順

The optical purity of (S)-β-phenylalanine was calculated from the peak area of the chromatogram obtained under analysis conditions illustrated in (1) above. Furthermore, the reaction yield of (S)-β-phenylalaninewas calculated from the peak area of the chromatogram obtained under analysis conditions illustrated in (2) above. Concretely, when the reaction solution contained a solid of β-phenylalanine or a solid of L-phenylalanine, a solution obtained by collecting a part of the reaction solution containing these solids, mixing with a 0.2 mol/l hydrochloric acid solution and dissolving these solids was analyzed. The amount (g) of (S)-β-phenylalanine synthesized was calculated from the peak area of the chromatogram using a calibration curve of (S)-β-phenylalanine standards to determine the yield from (Formula 1). Yield (%)=Amount of (S)-β-phenylalanine synthesized (g)/Amount of L-phenylalanine added (g)×100  (Formula 1)

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US08895270B2
出典データセットuspto-grants-2014_11
ORD IDord-0819d9f57f5d4c14aba814481d948dd0
出典メモuspto-grants-2014_11