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2-Hydrazinyl-4-iodopyridine → HCID 178453093、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Hydrazinyl-4-iodopyridine | HCID 53402897 | — |
| 反応物 | Tert-butyl (1-(2-formylquinolin-8-yl)piperidin-4-yl)methylcarbamate | HCID 86654345 | — |
| 溶媒 | Dichloromethane | HCID 6344 | — |
| 生成物 | HCID 178453093 | HCID 178453093 | — |
反応手順
To tert-butyl(1-(2-formylquinolin-8-yl)piperidin-4-yl)methylcarbamate (112 mg, 0.303 mmol) in DCM (20 mL) was added 1-(4-iodopyridin-2-yl)hydrazine (78.4 mg, 0.333 mmol). The reaction mixture was stirred for 1 hour and then taken on to directly to the next step.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08895550B2 |
| 出典データセット | uspto-grants-2014_11 |
| ORD ID | ord-c588082a25004edcb3c15d80b75b33fc |
| 出典メモ | uspto-grants-2014_11 |