関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Tetraethyl orthocarbonate | HCID 66213 | — |
| 反応物 | Biphenyl-4-yl-(3-hydroxyoxetan-3-yl)methanesulfonamide | HCID 68359244 | — |
| 溶媒 | Acetic Acid | HCID 176 | — |
| 生成物 | HCID 68292566 | HCID 68292566 | — |
反応手順
A mixture of 0.17 g of biphenyl-4-yl-(3-hydroxyoxetan-3-yl)methanesulfonamide in 4 ml of tetraethoxymethane and 1 ml of acetic acid was stirred at 90° C. for 3 hours. The solvent was removed under reduced pressure. This gave the crude product, which was used without further purification.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US08895547B2 |
|---|
| 出典データセット | uspto-grants-2014_11 |
|---|
| ORD ID | ord-c6b9c90066244e549bc33fd27109c190 |
|---|
| 出典メモ | uspto-grants-2014_11 |
|---|
