化工社化工社 化学情報印刷レポート · 研究参考用
(Phenylmethyl)hydrazine → 2-benzyl-5-(2-naphthyl)-2H-pyrazol-3-ylamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | (Phenylmethyl)hydrazine | HCID 11157 | — |
| 反応物 | beta-Oxo-2-naphthalenepropanenitrile | HCID 222856 | — |
| 生成物 | 2-benzyl-5-(2-naphthyl)-2H-pyrazol-3-ylamine | HCID 23070133 | — |
反応手順
900 mg of 2-benzyl-5-(2-naphthyl)-2H-pyrazol-3-ylamine obtained from 3-(naphthalen-2-yl)-3-oxopropionitrile and benzyl hydrazine in the similar method as described in Production example 30 was subjected to the similar reaction as described in Production example 31, to afford 770 mg of the title compound as a pale yellow powder.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07429609B2 |
| 出典データセット | uspto-grants-2008_09 |
| ORD ID | ord-7483e6c6f8f1442d9708eba5f6da490e |
| 出典メモ | uspto-grants-2008_09 |