関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Hydrazine hydrate (1:1) | HCID 24654 | — |
| 反応物 | 1-Piperidineacetic acid, ethyl ester | HCID 643466 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | 2-(Piperidin-1-yl)acetohydrazide | HCID 6421769 | — |
反応手順
3.86 g of piperidin-1-yl-acetic acid ethyl ester was dissolved in 40 mL of ethanol, added with 3.39 mL of hydrazine monohydrate, and stirred at 70° C. for 5 hours. After allowing the solution to cool to room temperature, the solvent was evaporated, to afford 3.8 g of the title compound as pale yellow crystals.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US07429609B2 |
|---|
| 出典データセット | uspto-grants-2008_09 |
|---|
| ORD ID | ord-c7ae76d9cb824d00b70c01074d2b137b |
|---|
| 出典メモ | uspto-grants-2008_09 |
|---|
