化工社化工社 化学情報印刷レポート · 研究参考用
Thionyl Chloride → 3-(Chlorocarbonyl)phenyl acetate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 反応物 | 3-Acetoxybenzoic acid | HCID 238669 | — |
| 生成物 | 3-(Chlorocarbonyl)phenyl acetate | HCID 12998558 | 99% |
反応手順
Using the above procedure, reaction of with thionyl chloride (11.1 mL, 15.3 mmol) and 3-acetoxybenzoic acid (2.50 g, 13.9 mmol) gave 511 (2.72 g, 99%) as a colorless oil. This material was used in the next step without additional purification.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08895752B2 |
| 出典データセット | uspto-grants-2014_11 |
| ORD ID | ord-0532de99dffc4e219aa9a7c1fb11c578 |
| 出典メモ | uspto-grants-2014_11 |