化工社化工社 化学情報印刷レポート · 研究参考用
N-ethyl-3-methylaniline → Propanamide, N-ethyl-N-(3-methylphenyl)-
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | N-ethyl-3-methylaniline | HCID 7603 | — |
| 反応物 | Propionyl chloride | HCID 62324 | — |
| 生成物 | Propanamide, N-ethyl-N-(3-methylphenyl)- | HCID 44150680 | — |
反応手順
N-Ethyl-N-(3-methylphenyl)propionamide was prepared on a laboratory scale by acylation of N-ethyl-m-toluidine with propionyl chloride. The reaction was carried out in a 5 litre 3 necked round bottomed flask equipped with a mechanical stirrer, a thermometer (0°-250° C.), an addition vessel and a condenser.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05856295 |
| 出典データセット | uspto-grants-1999_01 |
| ORD ID | ord-b8e167a762884ac4981728f815e679c1 |
| 出典メモ | uspto-grants-1999_01 |