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Oxalyl chloride → 3-[1-(2-propyl)-6-methoxymethyl-1H-indol-3-yl]-4-(1-methyl-1H-indol-3-yl)-pyrrole-2,5-dione
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Oxalyl chloride | HCID 65578 | — |
| 反応物 | Isopropyl 1-methyl-3-indoleacetimidate hydrochloride | HCID 22907276 | — |
| 反応物 | 6-Methoxymethyl-1-(2-propyl)indole | HCID 54229564 | — |
| 生成物 | 3-[1-(2-propyl)-6-methoxymethyl-1H-indol-3-yl]-4-(1-methyl-1H-indol-3-yl)-pyrrole-2,5-dione | HCID 17895481 | — |
反応手順
6-Methoxymethyl-1-(2-propyl)indole was reacted with oxalyl chloride and then 2-(1-methyl-1H-indol-3-yl) ethanimidic acid isopropyl ester hydrochloride as described in Example 3b to yield 3-[1-(2-propyl)-6-methoxymethyl-1H-indol-3-yl]-4-(1-methyl-1H-indol-3-yl)-pyrrole-2,5-dione.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05856517 |
| 出典データセット | uspto-grants-1999_01 |
| ORD ID | ord-f239dbe9b161478ebb17477ebbb2370b |
| 出典メモ | uspto-grants-1999_01 |