化工社化工社 化学情報印刷レポート · 研究参考用
Sulfuric Acid → DETA Epichlorohydrin
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sulfuric Acid | HCID 1118 | — |
| 反応物 | N,N-diethyl-m-toluamide | HCID 4284 | — |
| 反応物 | Epichlorohydrin | HCID 7835 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | DETA Epichlorohydrin | HCID 131721069 | — |
反応手順
To prepare the resin, the first portion of water is charged to a clean, dry, glass-lined reactor and the DMG-DETA base prepared as described above is added. The epichlorohydrin is added. The reaction solution is heated to 115°-120° F. Once the batch has reached between Gardner-Holdt "A" and "J", and preferably at "F", the second water and sulfuric acid are added. The preservative is then added. The pH is adjusted to 4.5±0.5 with DETA or sulfuric acid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05858171 |
| 出典データセット | uspto-grants-1999_01 |
| ORD ID | ord-bc957a7836804e94b3b5f20065693477 |
| 出典メモ | uspto-grants-1999_01 |