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2,6-Dichloro-3-methylaniline → N-(2,6-Dichloro-3-methylphenyl)-4,6-dimethyl-2-pyrimidinesulfonamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2,6-Dichloro-3-methylaniline | HCID 116529 | — |
| 反応物 | 4,6-Dimethylpyrimidine-2-sulfonyl fluoride | HCID 14404718 | — |
| 生成物 | N-(2,6-Dichloro-3-methylphenyl)-4,6-dimethyl-2-pyrimidinesulfonamide | HCID 14404704 | — |
反応手順
This material was prepared from 2,6-dichloro-3-methylaniline and 4,6-dimethyl-2-pyrimidinesulfonyl fluoride following the general procedure described in Example 2. The desired product was isolated as a solid, m.p. 234°-235°. NMR (90 MHZ) D6 -Acetone: δ 7.4 (d, 2H), 7.3 (s, 1H), 2.5 (s, 6H) and 2.3 (s, 3H).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04761173 |
| 出典データセット | uspto-grants-1988_08 |
| ORD ID | ord-ecd2f98b80d3423c9e2f3a399d300e50 |
| 出典メモ | uspto-grants-1988_08 |