Dimethylformamide → 7-Methoxyheptanoic Acid
反応式
Br[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][C:8]([OH:10])=[O:9].CN(C)[CH:13]=[O:14]>>[CH3:13][O:14][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][C:8]([OH:10])=[O:9]参加物
3
実験手順
The title compound was prepared by the method of Example 1 using 7-bromoheptanoic acid (50 g, 239 mmol) instead of 12-bromoundecanoic acid and dimethylformamide (300 mL) instead of methanol as the solvent. Concentration afforded the title compound (30 g) as a pale yellow liquid and the structure verified by NMR.
後処理
- concentrationConcentration
出典と根拠
- ORDレコード
- ord-3a5037c1041c4a34adf0fcfe5e2c122c
- 出典データセット
- uspto-grants-1999_01
- 特許番号
- US05859052
反応ノート
読み込み中…