化工社化工社 化学情報印刷レポート · 研究参考用
Benzaldehyde → Ethyl 2-benzylideneaminobutyrate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzaldehyde | HCID 240 | — |
| 反応物 | Triethylamine | HCID 8471 | — |
| 反応物 | Ethyl 2-Aminobutyrate Hydrochloride | HCID 12844023 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | Ethyl 2-benzylideneaminobutyrate | HCID 10331026 | — |
反応手順
Triethylamine (2 moles) was added to a solution of the product from step (a) (1 mole) in toluene. When addition was complete, benzaldehyde (1 mole) was added. The mixture was azeotroped until no further water was collected, then cooled to room temperature and filtered. The filtrate was evaporated in vacuo ti give the desired product as an oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05859240 |
| 出典データセット | uspto-grants-1999_01 |
| ORD ID | ord-410984a921a147c6bb9ce5296f537673 |
| 出典メモ | uspto-grants-1999_01 |