反応式
[CH3:1][CH:2]([CH:6]([CH3:10])[C:7]([OH:9])=[O:8])[C:3](O)=[O:4].C(Cl)(=O)C>>[CH3:1][CH:2]1[CH:6]([CH3:10])[C:7](=[O:9])[O:8][C:3]1=[O:4]参加物
3
反応条件
- 温度
- 65 °C
実験手順
To the 2,3-dimethyl succinic acid (5.13 g, 35.1 mmol), was added acetyl chloride (8.27 g, 7.49 mL, 105 mmol) at room temperature. The reaction mixture was refluxed at about 65° C. for 2 hrs. Workup consisted of concentration in vacuo, and drying in high vacuo. The desired product (4.95 g, with a little impurity of acetic acid) was obtained as a white solid.
後処理
- concentrationWorkup consisted of concentration in vacuo
- customdrying in high vacuo
出典と根拠
- ORDレコード
- ord-57939b2bc3864ae9a6026904999a5656
- 出典データセット
- uspto-grants-1999_01
- 特許番号
- US05861428
関連ノート
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