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N-[2-(3,4-Dichlorophenyl)-4-oxobutyl]-N-methylbenzamide → N-Methylbenzamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | N-[2-(3,4-Dichlorophenyl)-4-oxobutyl]-N-methylbenzamide | HCID 22137499 | — |
| 反応物 | 4-[(2,2,2-Trifluoroacetyl)[2-(2,2,2-trifluoroacetylamino)ethyl]amino]piperidine | HCID 22137541 | — |
| 反応物 | (S)-N-[2-(3,4-Dichlorophenyl)-4-[4-[(2,2,2-trifluoro-acetyl)[2-(2,2,2-trifluoroacetylamino)ethyl]amino]piperidino]-butyl]-N-methylbenzamide | HCID 54511194 | — |
| 生成物 | N-Methylbenzamide | HCID 11954 | — |
反応手順
(S)-N-[2-(3,4-Dichlorophenyl)-4-[4-[(2,2,2-trifluoroacetyl)[2-(2,2,2-trifluoroacetylamino)ethyl]amino]piperidino]-butyl]-N-methylbenzamide. Using the procedure of Example 1, replacing 4-(2-oxo-1,3-oxazolidin-3-yl)piperidine with 4-[(2,2,2-trifluoroacetyl)[2-(2,2,2-trifluoroacetylamino)ethyl]amino]piperidine, and N-[-2-(3,4-dichlorophenyl)-4-oxobutyl]-N-methylbenzamide with the (S)-enantiomer, the N-methylbenzamide was obtained as a viscous oil; MS: m/z=669(M+1).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05861392 |
| 出典データセット | uspto-grants-1999_01 |
| ORD ID | ord-45c91469529a4707a02864e3e6816034 |
| 出典メモ | uspto-grants-1999_01 |