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HRID 343724作成日:2026年10月27日

Acetate → HCID 66870991、化合物

https://huagongshe.com/reaction/343724

反応式

関与物質

役割名称HCID仕込み量
反応物AcetateHCID 175—
反応物Terephthalic AcidHCID 7489—
反応物Formic acid, copper saltHCID 44152240—
溶媒MethanolHCID 887—
生成物HCID 66870991HCID 6687099142.4%

反応手順

0.70 g of terephthalic acid was dissolved under heating in a mixture solvent of 400 cm3 of methanol and 20 cm3 of acetate. After this solution was cooled to the normal temperature, into this solution, a further solution in which 0.95 g of formic acid copper was dissolved in 50 cm3 of methanol was dripped and then this was kept still for a few days. Thereafter, the precipitation product was suction-filtered and dried for 110° C./4 hours, whereby 0.41 g of terephthalic acid copper was obtained.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US05862796
出典データセットuspto-grants-1999_01
ORD IDord-2efe6cc6b2654276953f915ae4f9b642
出典メモuspto-grants-1999_01