反応式
[C:1]([OH:8])(=[O:7])/[CH:2]=[CH:3]/[C:4]([OH:6])=[O:5].C(O)=O.[Cu:12].C(O)=O>CO>[Cu:12].[C:1]([OH:8])(=[O:7])/[CH:2]=[CH:3]/[C:4]([OH:6])=[O:5]参加物
5
実験手順
1.74 g of fumaric acid was dissolved in a mixture solvent having 100 cm3 of methanol and 8 cm3 of formic acid. Then, under stirring at the normal temperature, into the above solution, a further solution in which 3.38 g of formic acid copper was dissolved in 100 cm3 of methanol was dripped. After this solution was left still for one day, the precipitation product was suction-filtered and dried for 120° C./4 hours, whereby 1.23 g of fumaric acid copper was obtained. This substance had the specific surface area of 480 m2 /g.
後処理
- filtrationthe precipitation product was suction-filtered
- customdried for 120° C./4 hours
出典と根拠
- ORDレコード
- ord-aa4934b717674c5d9fe39db460c9e43a
- 出典データセット
- uspto-grants-1999_01
- 特許番号
- US05862796
関連ノート
読み込み中…