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HRID 343731作成日:2026年10月27日

Formic Acid → HCID 178525732、化合物

https://huagongshe.com/reaction/343731

反応式

関与物質

役割名称HCID仕込み量
反応物Formic AcidHCID 284—
反応物Formic acid, copper saltHCID 44152240—
反応物HCID 178525731HCID 178525731—
溶媒MethanolHCID 887—
生成物HCID 178525732HCID 17852573240.5%

反応手順

2.58 g of 1,4-trans-cyclohexane dicarboxylic acid was dissolved under heating in a mixture solvent of 100 cm3 of methanol and 20 cm3 of formic acid. After this solution was cooled to the normal temperature, into this solution under stirring, a further solution in which 3.38 g of formic acid copper was dissolved in 100 cm3 of methanol was dripped and then this was kept still for a few days. Thereafter, the precipitation product was suction-filtered and dried for 110° C./4 hours, whereby 1.43 g of 1,4-trans-cyclohexane dicarboxylic acid copper was obtained.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US05862796
出典データセットuspto-grants-1999_01
ORD IDord-c01f4852e5434038b46b74957eb732e9
出典メモuspto-grants-1999_01