化工社化工社 化学情報印刷レポート · 研究参考用
Formic Acid → HCID 178525732、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Formic Acid | HCID 284 | — |
| 反応物 | Formic acid, copper salt | HCID 44152240 | — |
| 反応物 | HCID 178525731 | HCID 178525731 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | HCID 178525732 | HCID 178525732 | 40.5% |
反応手順
2.58 g of 1,4-trans-cyclohexane dicarboxylic acid was dissolved under heating in a mixture solvent of 100 cm3 of methanol and 20 cm3 of formic acid. After this solution was cooled to the normal temperature, into this solution under stirring, a further solution in which 3.38 g of formic acid copper was dissolved in 100 cm3 of methanol was dripped and then this was kept still for a few days. Thereafter, the precipitation product was suction-filtered and dried for 110° C./4 hours, whereby 1.43 g of 1,4-trans-cyclohexane dicarboxylic acid copper was obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05862796 |
| 出典データセット | uspto-grants-1999_01 |
| ORD ID | ord-c01f4852e5434038b46b74957eb732e9 |
| 出典メモ | uspto-grants-1999_01 |