化工社化工社 化学情報印刷レポート · 研究参考用
Allyl bromide → N-(2-allyl-3-hydroxy-4-methylphenyl)-3,4,5,6-tetrahydrophthalimide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Allyl bromide | HCID 7841 | — |
| 反応物 | 2-Chloro-5-nitrophenol | HCID 69264 | — |
| 反応物 | 2-Methyl-5-nitrophenol | HCID 93576 | — |
| 反応物 | N-(2-allyl-4-chloro-3-hydroxyphenyl)-3,4,5,6-tetrahydrophthalimide | HCID 57171405 | — |
| 生成物 | N-(2-allyl-3-hydroxy-4-methylphenyl)-3,4,5,6-tetrahydrophthalimide | HCID 57199273 | — |
反応手順
N-(2-allyl-3-hydroxy-4-methylphenyl)-3,4,5,6-tetrahydrophthalimide (5A) was prepared, as yellow crystals, m.p.: 141°-143° C., from 2-methyl-5-nitrophenol and allyl bromide by the procedures described in Example 3 for preparing 3D from 2-chloro-5-nitrophenol and allyl bromide.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05053071 |
| 出典データセット | uspto-grants-1991_10 |
| ORD ID | ord-1003bfc266a2469b9b83c5d074b97f6e |
| 出典メモ | uspto-grants-1991_10 |