化工社化工社 化学情報印刷レポート · 研究参考用
Oxalyl chloride → Oleoyl chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Oxalyl chloride | HCID 65578 | — |
| 反応物 | Oleic Acid | HCID 445639 | — |
| 溶媒 | Hexane | HCID 8058 | — |
| 生成物 | Oleoyl chloride | HCID 5364783 | — |
反応手順
A 1.0 g portion of oleic acid was dissolved in 10 ml of hexane. A 2.0 ml portion of oxalyl chloride was added and this mixture was stirred under dry conditions for 1.5 hours, then evaporated in vacuo, giving the desired compound as a colorless oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05053426 |
| 出典データセット | uspto-grants-1991_10 |
| ORD ID | ord-cb048427a94349fe96c65f45efcdb2bf |
| 出典メモ | uspto-grants-1991_10 |