化工社化工社 化学情報印刷レポート · 研究参考用
Vinyl valerate → 4-(Tetrahydropyran-2-yloxy)phenylethanol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Vinyl valerate | HCID 62497 | — |
| 反応物 | 1-(4-(1-Ethoxyethoxy)phenyl)ethyl butyrate | HCID 54484855 | — |
| 生成物 | Ethyl valerate | HCID 10882 | 91% |
| 生成物 | 4-(Tetrahydropyran-2-yloxy)phenylethanol | HCID 53947316 | 94% |
反応手順
The procedure of Example 5 (i) was repeated except that vinyl valerate was used instead of 2,2,2-trichloroethyl butyrate to give 10.4 g of S-form of 1-(4-(tetrahydro-2-pyranyloxy)phenyl)ethanol (yield: 94%) and 13.9 g of R-form of 1-(4-tetrahydro-2-pyranyloxy)phenyl)ethyl valerate (yield: 91%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05053507 |
| 出典データセット | uspto-grants-1991_10 |
| ORD ID | ord-0c957c8c3ca3414f86d57079df14e812 |
| 出典メモ | uspto-grants-1991_10 |