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HRID 34485作成日:2026年10月26日

2,2,6,6-Tetramethylpiperidine → 5-Hexene-2,4-dione, 6-phenyl-

https://huagongshe.com/reaction/34485

反応式

関与物質

役割名称HCID仕込み量
反応物2,2,6,6-TetramethylpiperidineHCID 13035—
反応物AcetylacetoneHCID 31261—
溶媒TriethylamineHCID 8471—
生成物5-Hexene-2,4-dione, 6-phenyl-HCID 2784859—

反応手順

The title compound was prepared by the method of Example 6 (that is, using 2,2,6,6-tetramethylpiperidine as base instead of triethylamine) using 2,4-pentanedione instead of ethyl acetoacetate. The material prepared by this procedure was identical to that prepared by the method of Example 30, as indicated by the reverse phase chromatographic method described in Example 2.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04761503
出典データセットuspto-grants-1988_08
ORD IDord-7a2e1349a9674e6e93d465cf501a1fb5
出典メモuspto-grants-1988_08