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Dicyclohexylcarbodiimide → HCID 178444553、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dicyclohexylcarbodiimide | HCID 10868 | — |
| 反応物 | 4-Hydroxyphenylsulfur pentafluoride | HCID 2779203 | — |
| 反応物 | HCID 178444557 | HCID 178444557 | — |
| 溶媒 | Dichloromethane | HCID 6344 | — |
| 生成物 | HCID 178444553 | HCID 178444553 | — |
反応手順
A mixture of 10.6 g of dicyclohexylcarbodiimide and 40 ml of methylene chloride is added to a mixture of 9.1 g of trans-4-pentylcyclohexylcarboxylic acid, 11.2 g of p-hydroxyphenyl-sulfur pentafluoride and 100 ml of methylene chloride, and the combined mixture is heated at the boil for 6 hours. Working up in the customary manner gives 4-(trans-4-pentylcyclohexylcarbonyloxy)-phenyl-sulfur pentafluoride.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05055223 |
| 出典データセット | uspto-grants-1991_10 |
| ORD ID | ord-f36d29740ac64520a38116d18d5930db |
| 出典メモ | uspto-grants-1991_10 |