化工社化工社 化学情報印刷レポート · 研究参考用
Hydrogen Peroxide → Hydroxyethylacrylate Acrylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrogen Peroxide | HCID 784 | — |
| 反応物 | Thioglycolic Acid | HCID 1133 | — |
| 反応物 | Acrylic Acid | HCID 6581 | — |
| 反応物 | 2-Hydroxyethyl acrylate | HCID 13165 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Hydroxyethylacrylate Acrylate | HCID 86742315 | — |
反応手順
Acrylic acid (8.53%), hydroxyethylacrylate (2.84%) and water (31%) were charged to a reaction vessel placed under a nitrogen atmosphere. Thioglycolic acid (1.8%) and 35% aqueous hydrogen peroxide (1.8%) were charged with mixing to the same vessel with flushing between charges. At the completion of the exotherm. Sodium hydroxide (6.4%) aqueous was added with the stirring while maintaining a temperature below 70° C. Seven percent water is added and the material mixed further to produce Composition A.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04762626 |
| 出典データセット | uspto-grants-1988_08 |
| ORD ID | ord-3ecbbbf028514ad8b8b0fc5bf3934a4a |
| 出典メモ | uspto-grants-1988_08 |