化工社化工社 化学情報印刷レポート · 研究参考用
1-Adamantanol → 1-Adamantyl 2-(p-nitrophenyl)propionate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Adamantanol | HCID 64152 | — |
| 反応物 | 2-(4-Nitrophenyl)propionic acid | HCID 89244 | — |
| 反応物 | 1-Methylcyclohexyl 2-(p-nitrophenyl)propionate | HCID 54068492 | — |
| 生成物 | 1-Adamantyl 2-(p-nitrophenyl)propionate | HCID 21298167 | 92% |
反応手順
Using a method similar to that used in the preparation of 1-methylcyclohexyl 2-(p-nitrophenyl)propionate, 14.6 g of 2-(p-nitrophenyl)propionic acid, but using 1-adamantol instead of 1-methylcyclohexanol, were reacted to obtain 22.74 g (92% yield) of 1-adamantyl 2-(p-nitrophenyl)propionate as a light yellow viscous liquid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04762840 |
| 出典データセット | uspto-grants-1988_08 |
| ORD ID | ord-c5b67b715fb843d8baa6939c205a5268 |
| 出典メモ | uspto-grants-1988_08 |