2-(Methylamino)ethanol → N-Methyl-N-(3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraenoyl)-ethanolamin

HRID 34564

反応式

HRID 34564 の反応式
[CH3:1][C:2]([CH2:7][CH2:8][CH:9]=[C:10]([CH3:22])[CH2:11][CH2:12][CH:13]=[C:14]([CH3:21])[CH2:15][CH2:16][CH:17]=[C:18]([CH3:20])[CH3:19])=[CH:3][C:4]([OH:6])=O.[CH3:23][NH:24][CH2:25][CH2:26][OH:27]>>[CH3:23][N:24]([C:4](=[O:6])[CH:3]=[C:2]([CH3:1])[CH2:7][CH2:8][CH:9]=[C:10]([CH3:22])[CH2:11][CH2:12][CH:13]=[C:14]([CH3:21])[CH2:15][CH2:16][CH:17]=[C:18]([CH3:20])[CH3:19])[CH2:25][CH2:26][OH:27]

参加物

3

反応物 2

HCID 80162-(Methylamino)ethanolHCID 1285703,7,11,15-Tetramethyl-2,6,10,14-hexadecatetraenic acid

生成物 1

HCID 54048398N-Methyl-N-(3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraenoyl)-ethanolamin収率 92%

実験手順

The procedure of Example 1 was repeated except that 6.1 g of 3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraenoic acid and 2.4 ml of N-methylethanolamine were used. 6.6 g (yield 92%) of the title compound was obtained as a colorless oil.

出典と根拠

ORDレコード
ord-d5106581954f4fe4a6f2c2f345dfca3c
出典データセット
uspto-grants-1988_08
特許番号
US04762829

関連ノート

読み込み中…