Potassium Carbonate → HCID 15069997、化合物
反応式
[CH3:1][N:2]1[O:9][CH2:8][CH:7]2[CH:3]1[CH2:4][N:5](C(OCC)=O)[CH2:6]2.C(=O)([O-])[O-].[K+].[K+]>O>[CH3:1][N:2]1[O:9][CH2:8][CH:7]2[CH:3]1[CH2:4][NH:5][CH2:6]2参加物
4
実験手順
13 g (65 mmol) of ethyl 2-methyl-3-oxa-2,7-diazabicyclo[3.3.0]octane-7-carboxylate are heated under reflux in 300 ml of water with 41 g of Ba(OH)2.8H2O overnight. Potassium carbonate is added, the barium carbonate which has precipitated out is filtered off with suction and the filtrate is extracted ten times with 100 ml of chloroform each time. The extract is dried over potassium carbonate and concentrated and the residue is distilled.
後処理
- customthe barium carbonate which has precipitated out
- filtrationis filtered off with suction
- extractionthe filtrate is extracted ten times with 100 ml of chloroform each time
- dry with materialThe extract is dried over potassium carbonate
- concentrationconcentrated
- distillationthe residue is distilled
出典と根拠
- ORDレコード
- ord-a828fc3c88c34e6b8ebe6da3da0e0ca3
- 出典データセット
- uspto-grants-1991_10
- 特許番号
- US05059597
反応ノート
読み込み中…