化工社化工社 化学情報印刷レポート · 研究参考用
Tridecanoic acid → Tridecanoyl chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Tridecanoic acid | HCID 12530 | — |
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 溶媒 | Benzene | HCID 241 | — |
| 生成物 | Tridecanoyl chloride | HCID 87288 | — |
反応手順
To a benzene solution containing 5.0 g (0.023 mol) of tridecanoic acid was added 25 g of thionyl chloride, followed by refluxing for 5 hours. The excess of thionyl chloride and benzene were removed by distillation to obtain tridecanoyl chloride.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05059628 |
| 出典データセット | uspto-grants-1991_10 |
| ORD ID | ord-b6fd7f8ab8d244baa08dccc98c1036ee |
| 出典メモ | uspto-grants-1991_10 |