化工社化工社 化学情報印刷レポート · 研究参考用
3-Phenoxybenzaldehyde → 5,5-Dimethyl-2-(3-phenoxyphenyl)-3-(4-phenylbutyl)-4-thiazolidinone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-Phenoxybenzaldehyde | HCID 38284 | — |
| 反応物 | 2-Mercapto-2-methylpropanoic acid | HCID 78421 | — |
| 反応物 | Benzenebutanamine | HCID 83242 | — |
| 溶媒 | Benzene | HCID 241 | — |
| 生成物 | 5,5-Dimethyl-2-(3-phenoxyphenyl)-3-(4-phenylbutyl)-4-thiazolidinone | HCID 19990602 | — |
反応手順
Using the procedures of Example 5, the title compound was prepared as a light yellow viscous oil (8.4 g, 65%) from 5.9 g (0.030 mole) of 3-phenoxybenzaldehyde (Fluka), 3.6 g (0.030 mole) of 2-mercapto-2-methylpropionic acid, and 4.6 g (0.030 mole) of 4-phenylbutylamine after refluxing in 250 ml of benzene overnight.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05061720 |
| 出典データセット | uspto-grants-1991_10 |
| ORD ID | ord-79c0bbcc9ca8426eb94a9eff610b6370 |
| 出典メモ | uspto-grants-1991_10 |