化工社化工社 化学情報印刷レポート · 研究参考用
Acetic Acid → 6-Methoxy-2-naphthylacetic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acetic Acid | HCID 176 | — |
| 反応物 | Ethanol | HCID 702 | — |
| 反応物 | Sulfuric Acid | HCID 1118 | — |
| 反応物 | 4-Methoxybenzaldehyde | HCID 31244 | — |
| 反応物 | Chloroform methanol water | HCID 21866399 | — |
| 生成物 | 6-Methoxy-2-naphthylacetic acid | HCID 32176 | — |
反応手順
The final products, i.e. the phospholipid-drug conjugates obtained at the end of step 6, were subjected to TLC analysis under the following conditions: Silica gel 60 on aluminum sheet. Eluent is chloroform:methanol:water (65:35:5 v/v). Indicator is a spray of the composition: 4-methoxybenzaldehyde (10 ml), absolute ethanol (200 ml), 98% sulfuric acid (10 ml) and glacial acetic acid (2 ml). The chromatogram is sprayed with the indicator and then charred at 100° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07173018B2 |
| 出典データセット | uspto-grants-2007_02 |
| ORD ID | ord-ebb8d678259740259b882bd91435c301 |
| 出典メモ | uspto-grants-2007_02 |