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HRID 346445作成日:2026年10月26日

Acetic Acid → 6-Methoxy-2-naphthylacetic acid

https://huagongshe.com/reaction/346445

反応式

関与物質

役割名称HCID仕込み量
反応物Acetic AcidHCID 176—
反応物EthanolHCID 702—
反応物Sulfuric AcidHCID 1118—
反応物4-MethoxybenzaldehydeHCID 31244—
反応物Chloroform methanol waterHCID 21866399—
生成物6-Methoxy-2-naphthylacetic acidHCID 32176—

反応手順

The final products, i.e. the phospholipid-drug conjugates obtained at the end of step 6, were subjected to TLC analysis under the following conditions: Silica gel 60 on aluminum sheet. Eluent is chloroform:methanol:water (65:35:5 v/v). Indicator is a spray of the composition: 4-methoxybenzaldehyde (10 ml), absolute ethanol (200 ml), 98% sulfuric acid (10 ml) and glacial acetic acid (2 ml). The chromatogram is sprayed with the indicator and then charred at 100° C.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US07173018B2
出典データセットuspto-grants-2007_02
ORD IDord-ebb8d678259740259b882bd91435c301
出典メモuspto-grants-2007_02