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Chloroform → 4,4-Diaminodiphenylmethane
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Chloroform | HCID 6212 | — |
| 反応物 | Methyl Ethyl Ketone | HCID 6569 | — |
| 反応物 | N,2,2,6,6-Pentamethylpiperidin-4-amine | HCID 13657792 | — |
| 生成物 | 4,4-Diaminodiphenylmethane | HCID 7577 | — |
反応手順
3.58 g (0.03 mol) chloroform; 14.42 g (0.20 mol) 2-butanone; and, 4.0 g (0.1 mol) 4-methylamino-2,2,6,6-tetramethylpiperidine are reacted in a manner analogous to that described in Example 1 hereinabove and the product worked up and recovered. The structure of the compound obtained is represented as follows: ##STR5## wherein n is in the range from 2 to about 5.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04762872 |
| 出典データセット | uspto-grants-1988_08 |
| ORD ID | ord-d70ff801db8f481088cce50195ab3fba |
| 出典メモ | uspto-grants-1988_08 |