関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | 3-Methoxypropylamine | HCID 1672 | — |
| 反応物 | Quinizarin | HCID 6688 | — |
| 反応物 | Boric Acid | HCID 7628 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Quinizarin | HCID 6688 | — |
| 生成物 | 1,4-Dihydroxy-2-((3-methoxypropyl)amino)anthraquinone | HCID 88436 | — |
反応手順
2-(methoxypropylamino)-1,4-dihydroxyanthraquinone was prepared as follows: 60 grams of 1,4-dihydroxyanthraquinone, 15.5 grams of boric acid, and 89 grams of methoxypropylamine were slurried in 125 ml of water. The slurry was stirred and heated to 65° Celsius, and a strong stream of air was bubbled through it. These conditions were maintained about nine hours, or until thin layer chromatography of the reaction mixture failed to isolate any, 1,4-dihydroxyanthraquinone.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04764474 |
|---|
| 出典データセット | uspto-grants-1988_08 |
|---|
| ORD ID | ord-bdd196d979a84c5da73851f747171d88 |
|---|
| 出典メモ | uspto-grants-1988_08 |
|---|
